The Journal of Research of NIST and its predecessors report NIST research and development in metrology and related fields of: physical science, engineering, applied mathematics, statistics, biotechnology, information technology.
For additional information see: About the Journal
Volume 93 |
ISSN: 0160-1741 |
Issue 1 |
Issue 2 |
Issue 3 |
Issue 4 |
Issue 5 |
Issue 6 |
News briefs and reports, p. 1
http://dx.doi.org/10.6028/jres.093.002
The NBS scale of spectral irradiance, p. 7
http://dx.doi.org/10.6028/jres.093.003
Radiometric calibrations of portable sources in the vacuum ultraviolet, p. 21
http://dx.doi.org/10.6028/jres.093.004
Grid plate calibration at the National Bureau of Standards, p. 41
http://dx.doi.org/10.6028/jres.093.005
Phase meter calibration at NBS, p. 53
http://dx.doi.org/10.6028/jres.093.006
The application of flame spread theory to predict material performance, p. 61
http://dx.doi.org/10.6028/jres.093.007
Computer Security Conference - A Report on the 10th National Computer Security Conference, Baltimore, Md, September 21-24, 1987, p. 71
http://dx.doi.org/10.6028/jres.093.008
News briefs, p. 79
http://dx.doi.org/10.6028/jres.093.009
Measurement of the universal gas-constant R using a spherical acoustic resonator, p. 85
http://dx.doi.org/10.6028/jres.093.010
A computer-controlled data acquisition-system for combustion calorimetric experiments, p. 145
http://dx.doi.org/10.6028/jres.093.011
Partitioning of alkylbenzenes and aliphatic-alcohols between hexadecane and methanol-water mixtures, p. 161
http://dx.doi.org/10.6028/jres.093.012
Accuracy in Trace Analysis Accomplishments, Goals, Challenges September 28 - October 1, 1987 Gaithersburg, MD, Foreword
http://dx.doi.org/10.6028/jres.093.001
History of trace analysis, p. 175
http://dx.doi.org/10.6028/jres.093.013
Trace analysis by degrees - An academic perspective, p. 187
http://dx.doi.org/10.6028/jres.093.014
Importance of quantitative trace analysis in industry today, p. 189
http://dx.doi.org/10.6028/jres.093.015
The role of robotics in the laboratory of the 80s, p. 191
http://dx.doi.org/10.6028/jres.093.016
Chemometrics and standards, p. 193
http://dx.doi.org/10.6028/jres.093.017
Process analytical-chemistry, p. 207
http://dx.doi.org/10.6028/jres.093.018
Expert systems and robotics, p. 209
http://dx.doi.org/10.6028/jres.093.019
Accuracy in analysis - The role of standard reference materials, p. 213
http://dx.doi.org/10.6028/jres.093.020
Accuracy in trace analysis. II. Considerations of the measurement process. Quality assurance and reference materials for trace analysis, p. 217
http://dx.doi.org/10.6028/jres.093.021
Design of cost-effective QC procedures for clinical-chemistry assays, p. 218
http://dx.doi.org/10.6028/jres.093.022
Statistical-models in quality-control for trace analysis, p. 221
http://dx.doi.org/10.6028/jres.093.023
Quality-control in routine instrumental epithermal neutron-activation analysis of geological samples, p. 224
http://dx.doi.org/10.6028/jres.093.024
Importance of chemical blanks and chemical-yields in accurate trace chemical-analysis, p. 228
http://dx.doi.org/10.6028/jres.093.025
The importance of quality assurance in trace analysis, p. 232
http://dx.doi.org/10.6028/jres.093.026
A new river sediment standard reference material, p. 234
http://dx.doi.org/10.6028/jres.093.027
U.S. EPA reference standards and quality assurance materials for the analysis of environmental pollutants, p. 237
http://dx.doi.org/10.6028/jres.093.028
Characterization of high-purity silicides, p. 239
http://dx.doi.org/10.6028/jres.093.029
Accuracy in the determination of chlorinated dibenzo-para-dioxins and dibenzofurans in environmental-samples, p. 241
http://dx.doi.org/10.6028/jres.093.030
Pharmaceutical trace analysis, p. 242
http://dx.doi.org/10.6028/jres.093.031
Organic microanalysis of submicrogram samples, p. 245
http://dx.doi.org/10.6028/jres.093.032
Ethyl carbamate analysis in fermented products - A comparison of measurements of mass-spectrometry, thermal-energy analyzer, and hall electrolytic conductivity detector, p. 249
http://dx.doi.org/10.6028/jres.093.033
Multicomponent analysis in static and flow systems using digital-filters, p. 253
http://dx.doi.org/10.6028/jres.093.034
Evolutionary factor-analysis, p. 256
http://dx.doi.org/10.6028/jres.093.035
Chemometrics in Europe - Selected results, p. 257
http://dx.doi.org/10.6028/jres.093.036
Increased accuracy in the automated interpretation of large EPMA data sets by the use of an expert system, p. 260
http://dx.doi.org/10.6028/jres.093.037
Heteroscedastic calibration using analyzed reference materials as calibration standards, p. 264
http://dx.doi.org/10.6028/jres.093.038
The role of the robot in the chemical laboratory, p. 267
http://dx.doi.org/10.6028/jres.093.039
Laboratory robotics in radiation environments, p. 268
http://dx.doi.org/10.6028/jres.093.040
Microwave acid sample decomposition for elemental analysis, p. 269
http://dx.doi.org/10.6028/jres.093.041
Solid-phase extraction on a small-scale, p. 274
http://dx.doi.org/10.6028/jres.093.042
Determination of tributyltin in the marine-environment, p. 277
http://dx.doi.org/10.6028/jres.093.043
Analysis of gaseous and particle-associated PAH and nitroarenes in ambient air, p. 279
http://dx.doi.org/10.6028/jres.093.044
Pattern-recognition classification and identification of trace organic pollutants in ambient air from mass-spectra, p. 281
http://dx.doi.org/10.6028/jres.093.045
Annular denuders and filter packs designed to measure ambient levels of acidic and basic air-pollutants, p. 283
http://dx.doi.org/10.6028/jres.093.046
Measurement of sunlight-induced transient species in surface waters, p. 285
http://dx.doi.org/10.6028/jres.093.047
Trace radiocarbon analysis of environmental-samples, p. 289
http://dx.doi.org/10.6028/jres.093.048
The use of cryogenic size-reduction to improve purgeable priority pollutant analyses in soil samples, p. 292
http://dx.doi.org/10.6028/jres.093.049
Determination of 3-quinuclidinyl benzilate in urine, p. 293
http://dx.doi.org/10.6028/jres.093.050
Range-programming stripping voltammetry for determination of some metals in seawater, p. 296
http://dx.doi.org/10.6028/jres.093.051
Computer-assisted pesticide and PCB identification system (CAPPIS), p. 298
http://dx.doi.org/10.6028/jres.093.052
Sequential automated-analysis system for lower oxygenated organic-compounds in ambient air, p. 299
http://dx.doi.org/10.6028/jres.093.053
Trace level quantitation of phenyltin compounds using HPTLC, p. 301
http://dx.doi.org/10.6028/jres.093.054
Determination of chromium(III) and chromium(VI) by ammonium pyrrolidine dithiocarbamate-methyl isobutyl ketone-furnace atomic-absorption spectrometry, p. 305
http://dx.doi.org/10.6028/jres.093.055
Precision and bias of graphite-furnace analysis of environmental-samples, p. 307
http://dx.doi.org/10.6028/jres.093.056
An instrument for determination of energy oxygen and BOD5, p. 311
http://dx.doi.org/10.6028/jres.093.057
In situ filtration sampler for the measurement of trace-metals in precipitation, p. 312
http://dx.doi.org/10.6028/jres.093.058
Quantitation of arsenic species in urine for exposure assessment studies, p. 315
http://dx.doi.org/10.6028/jres.093.059
Biological reference materials for trace-element analysis - What is new, p. 318
http://dx.doi.org/10.6028/jres.093.060
Detecting contamination or trends in the concentrations of trace-metals in marine environments, p. 321
http://dx.doi.org/10.6028/jres.093.061
Determination of manganese in serum with Zeeman effect graphite-furnace atomic-absorption, p. 323
http://dx.doi.org/10.6028/jres.093.062
Appropriate reference parameters for the evaluation of elemental analysis data from biomedical specimens, p. 326
http://dx.doi.org/10.6028/jres.093.063
Ultra-trace elemental and isotopic quantification for neonatal nutrition studies, p. 328
http://dx.doi.org/10.6028/jres.093.064
Use of high-resolution GC/MS for obtaining accuracy in lipid measurements, p. 331
http://dx.doi.org/10.6028/jres.093.065
Some atomic-absorption spectrometric applications to clinical-biomedical trace-metal analyses, p. 334
http://dx.doi.org/10.6028/jres.093.066
Inaccuracies in clinical chemical-analysis, p. 336
http://dx.doi.org/10.6028/jres.093.067
Technical difficulties associated with the formation of C-11 labeled carboxylic-acids, p. 338
http://dx.doi.org/10.6028/jres.093.068
The development of definitive methods for organic serum constituents, p. 341
http://dx.doi.org/10.6028/jres.093.069
Recent advances in the analysis of PCBs and pesticides in human adipose-tissue, p. 343
http://dx.doi.org/10.6028/jres.093.070
Trace ultratrace analyses of unstable compounds - Investigations on hydrazobenzene and azobenzene, p. 344
http://dx.doi.org/10.6028/jres.093.071
Trace-element speciation in food - A combined enzymolysis SEC-ICP-MS approach, p. 349
http://dx.doi.org/10.6028/jres.093.072
Trace-element determinations in biologicals using atomic-absorption spectrometry, p. 350
http://dx.doi.org/10.6028/jres.093.073
Reliable measurement of major, minor, and trace elemental nutrients, p. 354
http://dx.doi.org/10.6028/jres.093.074
ICP-AES - a realistic assessment of its capabilities for food analysis, p. 358
http://dx.doi.org/10.6028/jres.093.075
Development of multi-purpose biological reference materials, p. 360
http://dx.doi.org/10.6028/jres.093.076
Accurate measurement of vitamins in foods and tissues, p. 362
http://dx.doi.org/10.6028/jres.093.077
Effects of ionizing-radiation on nutrients in foods, p. 364
http://dx.doi.org/10.6028/jres.093.078
Stable isotope-dilution GC MS for the quantification of food contaminants, p. 365
http://dx.doi.org/10.6028/jres.093.079
An isotope-dilution mass-spectrometric (IDMS) method for the determination of vitamin-C in milk, p. 367
http://dx.doi.org/10.6028/jres.093.080
Prospects for Trace Analysis in the Analytical Electron-Microscope, p. 369
http://dx.doi.org/10.6028/jres.093.081
Accuracy in microanalysis by electron energy-loss spectroscopy, p. 372
http://dx.doi.org/10.6028/jres.093.082
Analysis at the atomic level - The atom probe field-ion microscope, p. 374
http://dx.doi.org/10.6028/jres.093.083
Imaging microanalysis of materials with a finely focused heavy-ion probe, p. 377
http://dx.doi.org/10.6028/jres.093.084
Synchrotron radiation excited fluorescence micro-analysis using a new imaging technique, p. 379
http://dx.doi.org/10.6028/jres.093.085
Direct solids analysis using sputter initiated resonance ionization spectroscopy (Siris), p. 383
http://dx.doi.org/10.6028/jres.093.086
The accuracy of surface-analyses, p. 387
http://dx.doi.org/10.6028/jres.093.087
Depth profiling of trace constituents using secondary ion mass-spectrometry, p. 390
http://dx.doi.org/10.6028/jres.093.088
Relative sensitivity and quantitation in glow-discharge mass-spectrometry - A progress report, p. 392
http://dx.doi.org/10.6028/jres.093.089
Applications of mass-spectrometry in polymer analysis - Use of GC-GC-high resolution MS to identify photodative and oxidative-degradation products of BPA-polycarbonate, p. 394
http://dx.doi.org/10.6028/jres.093.090
Analytical-chemistry and material purity in the semiconductor industry, p. 396
http://dx.doi.org/10.6028/jres.093.091
Determination of traces of uranium and thorium in microelectronics constituent materials, p. 398
http://dx.doi.org/10.6028/jres.093.092
Multitechnique approach to trace characterization of high-purity materials - Gallium, p. 400
http://dx.doi.org/10.6028/jres.093.093
Open tubular liquid-chromatography and the analysis of single neurons, p. 403
http://dx.doi.org/10.6028/jres.093.094
High-performance capillary electrophoresis, p. 406
http://dx.doi.org/10.6028/jres.093.095
Supercritical fluid chromatography - Application to trace analysis, p. 409
http://dx.doi.org/10.6028/jres.093.096
Ion chromatography - From anions to metals, p. 411
http://dx.doi.org/10.6028/jres.093.097
Quantification of toxic-chemicals in selected human-populations, p. 412
http://dx.doi.org/10.6028/jres.093.098
An evaluation of Jansson method to deconvolve overlapped gas-chromatographic peaks, p. 413
http://dx.doi.org/10.6028/jres.093.099
Inorganic trace analysis by isotope-dilution mass-spectrometry - New frontiers, p. 417
http://dx.doi.org/10.6028/jres.093.100
Applications of the reaction interface mass-spectrometer technique to the analysis of selected elements and nuclides from submicrogram quantities of biological macromolecules and xenobiotics, p. 419
http://dx.doi.org/10.6028/jres.093.102
Alkylation of DNA invivo - Development of analytical methodology for trace quantitative-analysis, p. 419
http://dx.doi.org/10.6028/jres.093.101
Ion mobility spectrometry after chromatography - Accomplishments, goals, challenges, p. 425
http://dx.doi.org/10.6028/jres.093.103
Quantitative aspects of glow-discharge mass-spectrometry, p. 426
http://dx.doi.org/10.6028/jres.093.104
Studies of limit of detection on 2,4,6-trinitrotoluene (TNT) by mass-spectrometry, p. 428
http://dx.doi.org/10.6028/jres.093.105
Absolute cross-section measurements in XQQ instruments - The NBS round robin, p. 431
http://dx.doi.org/10.6028/jres.093.106
Assessment of the analytical capabilities of inductively coupled plasma-mass spectrometry, p. 433
http://dx.doi.org/10.6028/jres.093.107
Fluorescence spectrometric determination of nonfluorescent compounds via molecular fragmentation, p. 437
http://dx.doi.org/10.6028/jres.093.108
Enhanced multidimensional luminescence measurements through cyclodextrin complexation, p. 438
http://dx.doi.org/10.6028/jres.093.109
High resolution nonlinear laser spectroscopy, p. 440
http://dx.doi.org/10.6028/jres.093.110
Trace analysis of aromatic-compounds in natural samples by Shpolskii spectroscopy, p. 441
http://dx.doi.org/10.6028/jres.093.111
Sodium taurocholate micelles in fluorometric analysis, p. 443
http://dx.doi.org/10.6028/jres.093.112
Accuracy in furnace atomic-absorption spectroscopy, p. 445
http://dx.doi.org/10.6028/jres.093.113
Microwave induced plasmas as sources for atomic spectrometry, p. 447
http://dx.doi.org/10.6028/jres.093.114
Graphite-furnace AAS - Application of reduced palladium as a chemical modifier, p. 450
http://dx.doi.org/10.6028/jres.093.115
The determination of trace-elements in uranium oxide (U3O8) by inductively coupled plasma emission-spectrometry and graphite-furnace atomic-absorption spectrometry, p. 452
http://dx.doi.org/10.6028/jres.093.116
ICP trace-element analyses from fusion dissolution, p. 454
http://dx.doi.org/10.6028/jres.093.117
Automation and application of a direct-current plasma emission spectrometer, p. 458
http://dx.doi.org/10.6028/jres.093.118
Flow injection inductively coupled plasma spectrometry - A new strategy for ultratrace analysis, p. 462
http://dx.doi.org/10.6028/jres.093.119
Some applications of isotope analysis of lead in food by ICP-MS, p. 464
http://dx.doi.org/10.6028/jres.093.120
Improving accuracy in graphite-furnace atomic-absorption spectrometry through peak shape monitoring, p. 467
http://dx.doi.org/10.6028/jres.093.121
Analysis of trace-elements in methamphetamine hydrochloride by inductively coupled plasma-mass spectrometry, p. 469
http://dx.doi.org/10.6028/jres.093.122
MeV ion-beam analysis, p. 473
http://dx.doi.org/10.6028/jres.093.123
Classical pitfalls in contemporary nuclear-data analysis, p. 479
http://dx.doi.org/10.6028/jres.093.124
A uniform concept for error estimation in gamma-ray spectrometry, p. 481
http://dx.doi.org/10.6028/jres.093.125
Accuracy in CPAA for C, N and O and in ERDA and NRA for H, p. 482
http://dx.doi.org/10.6028/jres.093.126
A fast-neutron diagnostic probe, p. 484
http://dx.doi.org/10.6028/jres.093.127
Trace analyses of impurities in povidone by square-wave voltammetry, p. 487
http://dx.doi.org/10.6028/jres.093.128
Voltammetric sensors using chemically active electrode materials, p. 488
http://dx.doi.org/10.6028/jres.093.129
Adsorptive stripping voltammetry - A new electroanalytical avenue for trace analysis, p. 489
http://dx.doi.org/10.6028/jres.093.130
Electrochemical enzyme-immunoassay, p. 491
http://dx.doi.org/10.6028/jres.093.131
Stripping voltammetric assay of trace technetium with a topo coated glassy-carbon electrode, p. 493
http://dx.doi.org/10.6028/jres.093.132
Electrochemical studies of dithiocarbamates and related-compounds, p. 496
http://dx.doi.org/10.6028/jres.093.133
Biochemical applications of chromatography/SIMS, p. 499
http://dx.doi.org/10.6028/jres.093.134
Chemi-luminescence detection in flowing streams - Immobilized and solid-state reagents, p. 501
http://dx.doi.org/10.6028/jres.093.135
Applications of lasers in bioanalytical chemistry, p. 502
http://dx.doi.org/10.6028/jres.093.136
Trace biogenic-amine analysis with pre-column derivatization and with fluorescent and chemi-luminescent detection in HPLC, p. 504
http://dx.doi.org/10.6028/jres.093.137
Homogeneous electrochemical immunoassay using a chemically modified electrode, p. 506
http://dx.doi.org/10.6028/jres.093.138
Accuracy in quantitative electron-probe microanalysis, p. 509
http://dx.doi.org/10.6028/jres.093.139
Quantitative secondary ion mass spectrometry, p. 510
http://dx.doi.org/10.6028/jres.093.140
Quantitative compositional mapping on a micrometer scale, p. 518
http://dx.doi.org/10.6028/jres.093.141
Transferring accuracy to the trace level and then to the field, p. 520
http://dx.doi.org/10.6028/jres.093.142
News briefs, p. 527
http://dx.doi.org/10.6028/jres.093.143
An Improvement in the reliability of standard cell enclosures, p. 533
http://dx.doi.org/10.6028/jres.093.144
The NBS vision system in the AMRF, p. 539
http://dx.doi.org/10.6028/jres.093.145
International comparisons of pressure standards: A status-report, p. 545
http://dx.doi.org/10.6028/jres.093.146
Condensation method for humidity measurement in the UMR cloud simulation chamber, p. 551
http://dx.doi.org/10.6028/jres.093.147
Precipitation of NH4UO2PO4.3H2O - Solubility and structural comparison with alkali uranyl(2+) phosphates, p. 557
http://dx.doi.org/10.6028/jres.093.148
Practical uncertainty limits to the mass determination of a piston-gage weight, p. 565
http://dx.doi.org/10.6028/jres.093.149
News briefs, p. 573
http://dx.doi.org/10.6028/jres.093.150
Diffraction imaging (topography) with monochromatic synchrotron radiation, p. 577
http://dx.doi.org/10.6028/jres.093.151
Convective velocity effects on a thermistor in water, p. 603
http://dx.doi.org/10.6028/jres.093.152
Octacalcium Phosphate Solubility Product from 4 to 37°C, p. 613
http://dx.doi.org/10.6028/jres.093.153
Surface Metrology - A Report on the 4th International Conference on the Metrology and Properties of Engineering Surfaces, National Bureau of Standards, Gaithersburg, MD, April 13-15, 1988, p. 625
http://dx.doi.org/10.6028/jres.093.154
The National Bureau of Standards becomes the National Institute of Standards and Technology, p. 635
http://dx.doi.org/10.6028/jres.093.155
News briefs, p. 637
http://dx.doi.org/10.6028/jres.093.156
Kinetic-studies using a highly sensitive microphone detector, p. 643
http://dx.doi.org/10.6028/jres.093.157
Solvent-free injection in supercritical fluid chromatography using sintered glass deposition, p. 655
http://dx.doi.org/10.6028/jres.093.158
Enzyme-enhanced electrochemical immunoassay for phenytoin, p. 659
http://dx.doi.org/10.6028/jres.093.159
Liposome-based flow-injection immunoassay system, p. 663
http://dx.doi.org/10.6028/jres.093.160
Workshop on Microstructure and Macromolecular Research With Cold Neutrons - National-Bureau-of-Standards, Gaithersburg, Md, April 21-22, 1988, p. 667
http://dx.doi.org/10.6028/jres.093.161
United States-Japan Panel on Wind and Seismic Effects - National Bureau of Standards, Gaithersburg, Md, May 17-20, 1988, p. 671
http://dx.doi.org/10.6028/jres.093.162

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