NIST has developed an organizational policy on traceability and a set of related supplementary materials, which includes answers to questions frequently asked by customers of NIST measurement services. The policy and supplementary materials are intended to serve as a resource for NIST customers.
I.A Questions about Metrological Traceability in General
The definition of traceability that has achieved global acceptance in the metrology community is contained in the International vocabulary of metrology - Basic and general concepts and associated terms : "…property of a measurement result whereby the result can be related to a reference through a documented unbroken chain of calibrations, each contributing to the measurement uncertainty
It is important to note that traceability is the property of the result of a measurement, not of an instrument or calibration report or laboratory. It is not achieved by following any one particular procedure or using special equipment. Merely having an instrument calibrated, even by NIST, is not enough to make the measurement result obtained from that instrument traceable to realizations of the appropriate SI unit or other specified references. The measurement system by which values and uncertainties are transferred must be clearly understood and under control.
Only measurement results are traceable.
Organizations cannot be traceable. Only measurement results can be traceable.
The provider of the result of a measurement is responsible for supporting its claim of the traceability of that result or value. This is the case whether that provider is NIST or another organization.
To support a claim, the provider of a measurement result must document the measurement process or system used to establish the claim and provide a description of the chain of calibrations that were used to establish a connection to a particular specified reference. There are several common elements to all valid statements or claims of traceability:
An internal measurement assurance program may be quite simple or very complex, the level or rigor to be determined depending on the level of uncertainty at issue and what is needed to demonstrate its credibility. Users of a measurement result are responsible for determining what is adequate to meet their needs.
For information and guidance on expressing measurement uncertainty, see http://physics.nist.gov/cuu/.
See Section V Checklist for Traceability through Calibration for additional guidance.
The user of the result of a measurement is responsible for assessing the validity of a claim of traceability. However, as discussed in Question I.A.4 above, the provider is responsible for providing the necessary information that the user assesses.
See Question I.A.5 above, which provides information on what the provider of a measurement result should do to support a claim of traceability. As a user, you should look for these elements. See Section V Checklist for Traceability through Calibration for additional guidance.
Per the VIM definition, metrological traceability is established through "an unbroken chain of calibrations, each contributing to the measurement uncertainty." In practical terms, this means having in place, for each link in the chain:
An internal measurement assurance program may be quite simple or very complex, the level or rigor to be determined depending on the level of uncertainty at issue and what is needed to demonstrate its credibility.Users of a measurement result are responsible for determining what is adequate to meet their needs.
For information and guidance on expressing measurement uncertainty, see http://physics.nist.gov/cuu/.
The provider of the result of a measurement is responsible for establishing the traceability of this result. This is the case whether that provider is NIST or another organization.
I.B.3 Does metrological traceability need to be reexamined periodically? What are the criteria for judging the integrity of the metrological traceability chain?
Yes, traceability does need to be reexamined periodically, and the criteria for assessing the integrity of the traceability chain are dependent on many things. To be considered are: the measurement requirements, the needs of the client, the dependability of the equipment and standards, the environmental effects, etc. For more details, see Reference .
Test report numbers issued by NIST are intended to be used solely for administrative purposes. Although they are often used to uniquely identify documents which bear evidence of traceability, test report numbers themselves do not address the issues listed in I.B.1 above, and should not be used nor required as the sole proof of traceability.
I.B.5 To establish the traceability of a measurement result for a particular measurand, is it also necessary to establish the traceability of all other values of measured quantities associated with the measurand, especially those that might contribute in a relatively minor way? For example, when making a dimensional measurement, do the measurements of barometric pressure, humidity, and temperature for a dimensional measurement need to be traceable to the International System of Units (SI)?
As a general principle, the definition of metrological traceability in the VIM suggests that it is necessary to establish the traceability of all associated input quantities in a measurement model. A measurement model defines the way in which a measurement result depends upon an associated input quantity. For example, a dimensional measurement result may depend upon barometric pressure, humidity, and temperature, if the value of, and/or the variation in these quantities contributes significantly to the value or stated uncertainty of the measurement result.
As a practical matter, the contribution of an input quantity to a measurement result is significant if a change in the value or uncertainty of the input quantity corresponds to a change in the significant figures of the stated value or uncertainty of the measurement result. When this is the case, traceability for the measurement of the associated input quantity should be established. The required levels of uncertainty that must be achieved for these associated input quantities may be relatively large, depending on the degree to which the input quantity actually affects the value or the stated uncertainty of the measurement result.
The National Institute of Standards and Technology (NIST) (http://www.nist.gov/) is an agency of the Department of Commerce. Its role as the National Metrology Institute (NMI) for the United States was established by Congress in 1901. As such, NIST has the responsibility "to develop, maintain and retain custody of the national standards of measurement, and to provide the means and methods for making measurements consistent with those standards; to assure the compatibility of United States national measurement standards with those standards; and to assure the compatibility of United States national measurement standards with those of other nations." [15 U.S.C. 271] The job of NIST is twofold: to ensure U.S. national standards are accurate realizations of the SI units and to transfer the values of those standards to the U.S. measurement system through calibrations and other types of measurement services. Direct customers of NIST’s measurement services take advantage of the opportunity to tie their internal measurement standards to NIST standards and hence, to the SI units. These companies, in turn, use their standards to provide measurement services to their customers, to meet regulatory requirements, and to provide quality assurance in their manufacturing processes. NIST also supports laboratories that provide calibrations through its National Voluntary Laboratory Accreditation Program (NVLAP). (see also Question I.D.2, next section, for information on NIST products and services)
NIST has various roles in traceability:
According to the internationally recognized VIM definition, metrological traceability is a property of a measurement result by which that result is related to specified reference standards, not to institutions. Accordingly, the phrase "traceable to NIST", in its most proper sense, is shorthand for "metrologically traceable to NIST's practical realization of the definition of a measurement unit" (see 2.43 in Reference ).
To achieve traceability of measurement results to standards maintained by NIST, you need to reference your measurement results through an unbroken chain of calibrations, including determining the uncertainties at each step, to NIST standards as the specified references. These references may be, for example, standards developed and maintained by NIST: broadcast signals controlled or monitored by NIST (such as standard time and frequency signals), NIST Standard Reference Materials (SRMs), or NIST-Traceable Reference Materials (NTRMs). The chain of calibrations may be short, if the user has instruments or artifacts calibrated by NIST or acquires standards from NIST and references measurement results to those. It may be longer, if the user references other calibrations in a chain of calibrations back to stated references developed and maintained by NIST. Also see Question I.A.5 above and Section V Checklist for Traceability through Calibration for additional guidance.
In general, NIST establishes the traceability of its own measurement results by following the prescription of the VIM definition of traceability, that is, through an unbroken chain of calibrations, including determining the uncertainties at each step, to specified references. In the case of the SI units, for six of the seven base units the ultimate stated reference is a CIPM-established definition of the units, including associated procedures; for one SI unit, mass, the reference is specified as the international prototype kilogram. The same process also applies in the case of derived units, which are formed as products of powers of the base units according to the algebraic relations linking the quantities concerned. For other measurement quantities, the reference may be a national standard defined de facto by a conventionally stated method.
NIST documents the process by which it establishes traceability of its own measurement results as part of the NIST System for Assuring Quality in the Results of Measurements Delivered to Customers in Calibration and Measurement Certificates (http://www.nist.gov/pml/nvlap/qualitysystem/). In accordance with the System, NIST maintains current technical descriptions of (a) the measurement facility, system, or methods; (b) the procedures for conduct of the measurement(s); (c) the analysis of uncertainty of the measurement results; and (d) the procedures for statistical control of the measurement process. This documentation includes a description of how traceability is/was achieved.
According to the NIST policy on traceability, NIST establishes the traceability of the results of its own measurements and of results provided to customers in NIST calibration and measurement certificates and, if not always explicitly then always by clear implication, certifies that traceability. Although the measurement results in a calibration or measurement certificate can be considered to be ‘certified’ by NIST to be traceable to NIST reference standards at the time the measurements were performed, NIST cannot ‘certify’ that those measurement results are valid after an instrument has left NIST. In the case of Standard Reference Materials, each certificate specifies the conditions under which NIST stands behind its measurement results after the SRM has left NIST. The customer must have an appropriate internal measurement assurance program in place to assure the continued validity of those measurement results. See Reference .
NIST only certifies the traceability of measurement results that NIST itself provides, either directly or through an official NIST program or collaboration. Some examples of such official NIST programs or collaborations are described in Section II Examples of NIST Programs in Traceability. NIST cannot be responsible for claims of traceability made by others since the process of demonstrating traceability requires that most of the steps be taken at the site of whoever is claiming traceability. NIST has no control over this process and no direct involvement in the day-to-day activities at the site. (See Section V Checklist for Traceability through Calibration for supporting a claim of traceability through calibration for an illustration of activities to be performed at a customer facility, as opposed to activities performed at a reference laboratory.)
I.C.9 Given that NIST operates the National Voluntary Laboratory Accreditation Program (NVLAP), does this mean that NIST stands behind claims of traceability made by NVLAP-accredited labs?
No, laboratory accreditation, whether conducted by NIST/NVLAP or any other recognized accreditation body, is a finding of a laboratory’s competence and capability to provide technically sound and appropriate measurement services within their scope of accreditation. Embedded in the process is an evaluation of the lab’s ability to achieve and maintain traceability for the accredited services. Accreditation to ISO/IEC 17025  determines that a laboratory has all of the necessary facilities, equipment, standards, procedures, uncertainty analyses, personnel, etc., which make it capable of providing traceable measurement results. Laboratory accreditation does not speak to the specifics of any individual measurement result but to the overall capability of a lab to provide the service. NIST experts often participate in the accreditation process, but again, the end result is a finding of competence and capability only.
Yes, NIST has a variety of publications. See references list in Section IV.
I.D.2 What products and services does NIST provide in support of customers seeking to establish traceability?
NIST provides a range of products and services in support of customers seeking to establish traceability of their measurement results. These include instrument calibrations, Standard Reference Materials (SRMs), and Standard Reference Data (SRD). NIST also provides measurement services to State and local governments responsible for marketplace transactions that involve measurements (weights and measures). NIST’s Calibration Program, Standard Reference Materials Program, and the Weights and Measures Program make up the largest integrated national measurement transfer system in the world. The Standard Reference Data Program augments this system by providing scientists, engineers and the general public with access to critically evaluated data necessary to perform state-of-the-art research and development. Through these four programs, NIST disseminates expert metrology guidance and the measurement products and services developed in the NIST Laboratories to the industrial and scientific communities, federal agencies and state and local governments.
Calibration laboratories and testing facilities may be accredited by NIST under the National Voluntary Laboratory Accreditation Program (NVLAP). The basic procedures and general accreditation requirements of NVLAP are described in Reference . A participating laboratory may voluntarily take steps to improve or assess its measurement process.
NIST Laboratories also provide a range of training courses and workshops on measurement practices. Topics covered include precision thermometry, temperature measurement by radiation thermometry, laser measurements, gage block calibration, time and frequency fundamentals, dimensional metrology, pressure, etc.
For information and guidance on expressing measurement uncertainty, see http://physics.nist.gov/cuu/.
I.D.3 If I have an instrument or artifact calibrated at NIST, does that make my measurement results traceable to those of NIST?
Merely having an instrument or artifact calibrated at NIST is not enough to make the measurement result traceable to reference standards developed and maintained by NIST. To establish traceability to such reference standards, there must be an unbroken chain of calibrations and each provided measurement must be accompanied by a statement of uncertainty. The measurement system by which values are transferred must be clearly understood and under control. The dates and details of each link in the chain must also be provided.
The purchase of an SRM does not automatically make the customer’s measurement results traceable to reference standards developed and maintained by NIST. NIST SRMs serve as one mechanism for achieving measurement compatibility based on accuracy, and are intended to be used as part of a measurement system or program. The guiding principle in issuing an SRM is that it is used for measurement quality assessment. A claim of traceability to reference standards developed and maintained by NIST can be asserted by proper use of appropriate SRMs and reference to the certified values and uncertainties provided by a NIST Certificate of Analysis. This Certificate contains a statement of the intended use of the SRM (NOTE: NIST cannot foresee all the uses for a specific SRM and recognizes that defensible assertions can be made for alternative use). In general, the Certificate also contains a disclaimer for improper handling of a material. It is up to the user to document appropriate storage and preservation of a material. An SRM certificate also contains an expiration date. It is inappropriate to use an expired material to establish a traceability claim. Finally, it is up to the user to demonstrate that the Certificate of Analysis in their possession is valid and up-to-date.
I.D.5 If I purchase a NIST Traceable Reference Material (NTRM), does that make my measurement results traceable to those of NIST?
As with SRMs, the purchase of an NTRM does not automatically make the customer’s measurement results traceable to reference standards developed and maintained by NIST. However, NTRMs can be used to make a claim of traceability to NIST in the same manner as SRMs, with reference to the certified values and uncertainties on an NTRM Certificate of Analysis.
I.D.6 NIST data are often used in claims of traceability to NIST. Under what conditions can one consider NIST data to be "specified references"?
NIST provides a number of data services that are critical to the measurement infrastructure of the United States and the world. These services include:
Great effort is made to describe clearly the type of data in NIST electronic and printed data collections. Usually, data from NIST are accompanied by uncertainties that have been estimated and propagated according to the Evaluation of measurement data - Guide to the expression of uncertainty in measurement (GUM) . When data are evaluated, the scientific basis used in evaluating these data is well documented and the data labeled as NIST Standard Reference Data.
The use of these data as "stated references" depends on the type of collection (Standard Reference Data, values of physical constants, etc.), the date of the most recent evaluation or compilation, and the direct relevance of the data to the physical measurement for which traceability is needed. In particular, if the data are not part of a NIST compilation of evaluated data, then care should be taken to assess the expressed uncertainty, and the literature checked for additional values for comparison.
I.D.7 Can organizations claim traceability to NIST by having individual instrument components calibrated at NIST? If so, is that the same as sending the entire instrument to NIST for calibration?
If the claim of traceability to reference standards developed and maintained by NIST is supported by an appropriate measurement assurance process and uncertainty analysis, the claim may be valid. The measurement process and uncertainty analysis must show how the basic component measurements are combined and translated into a complete calibration for the instrument in question. Is it the same as sending the complete instrument in? Possibly, but only when the organization combines the results using exactly the same measurement model and methods that NIST would use in calibrating the entire instrument, which is ordinarily not the case.
I.D.8 How should customers claim traceability to NIST if NIST needs to use two or more of its own standards to calibrate the customer instrument, standard, or artifact?
NIST may use a number of internal standards to calibrate or validate its own measurement process or system. The measurement results with associated uncertainties form the traceability link(s). The customer should claim traceability to the NIST system comprising the individual standards and should indicate who combined the data using what algorithm. Uncertainties should be documented, calculated, and reported accordingly.
I.D.9 Can customers claim traceability to NIST for measurement results associated with something that NIST cannot calibrate directly?
Yes, under certain circumstances. If well-accepted, scientifically sound and appropriate measurement equipment, practices, and procedures are used; if measurement values and uncertainties are calculated or otherwise established according to well-established protocols; and if the uncertainties are within accepted norms (both low and high) for the measurement application; then the customer's measurement result might be considered traceable to NIST.
As an example, there are many measurement quantities for which NIST does not offer calibration services, but that are derived from a combination of other measurement quantities for which NIST does provide calibration services. Torque is one example. NIST does not offer a calibration service for torque. It does, however, offer services for the component measurement quantities (mass, length, etc.) that are needed to derive torque, according to the well-accepted definition of torque. By performing the steps necessary to achieve traceability to NIST of the individual component measurement results when making a particular measurement of torque, it is possible to claim traceability of the corresponding measurement result to NIST. The uncertainty of the measurement result must first be calculated (again using a well-established methodology, such as that in NIST Technical Note 1297 ) using the uncertainties associated with the individual component measurement quantities. This uncertainty must be at (or above) a realistic level of uncertainty consistent with the sophistication of the measurement model and other practical and established considerations.
As another example, NIST does provide calibration services for voltage, but only at discrete values of voltage. If an organization wants to establish traceability to NIST at other values of voltage, it must develop an interpolation or extrapolation mechanism and protocol for doing this. Additional measurement uncertainties will result. The resulting statement of traceability must incorporate these additional uncertainties, which must again be realistic and within expected norms.
As a third example, NIST may not offer any calibration service or SRM for a particular measurement quantity, but may provide measurement protocols and advice, along with expected norms for levels of uncertainty that can be achieved according to the protocol. Under these circumstances, an organization may again claim traceability of its measurement results to NIST if the protocols (and built-in checks/tests) are followed, and the claimed uncertainties are within the expected norms.
For more on the "Elements of Traceability" please see clause 4 of Reference  and Reference .
The CIPM Mutual Recognition Arrangement (MRA) was drawn up by the International Committee of Weights and Measures (CIPM) under the authority given to it in the Metre Convention, for signature by directors of member National Metrology Institutes (NMIs). The principal objectives of the MRA are to establish through measurement comparisons the degree of equivalence of national measurement standards maintained by NMIs, to provide for the mutual recognition of calibration and measurement certificates issued by NMIs, and to provide a secure technical foundation for wider agreements related to international trade, commerce, and regulatory affairs. The mutual recognition of calibration and measurement certificates requires that each NMI participate in the activities of the International Bureau of Weights and Measures (BIPM) (including key measurement comparisons) and have a suitable way of assuring quality in the results of its measurement services. The results of the key measurement comparisons and specific statements of the calibration and measurement capabilities (CMCs) of each signatory NMI are entered in an MRA database originally developed by NIST and now maintained by the Bureau of International Weights and Measures at http://kcdb.bipm.org/.
While NIST recognizes the validity of the other signatories’ certificates, such recognition does not mean that measurement results traceable to any other signatory are therefore traceable to NIST. The burden of establishing traceability of its measurement results to NIST, and of supporting an associated claim of traceability, is on the individual NMI providing the service.
I.E.2 If a laboratory establishes traceability of its measurement results to standards maintained by National Metrology Institutes (NMIs) that is a signatory to the CIPM MRA, does that mean that that laboratory’s measurement results are traceable to standards maintained by other signatory NMIs?
While signatory NMIs (including NIST) recognize the validity of other signatories’ measurement and calibration certificates under the MRA, such recognition does not mean that measurement results obtained by one signatory NMI are automatically traceable to stated references developed and maintained by any other signatory NMI. However, users of measurement results, who may be either commercial or regulatory entities, may well decide that sufficient evidence exists under the MRA to provide mutually acceptable traceability of these results to the standards and measurements of two or more participating NMIs. Such evidence may include comparable claims of calibration and measurement capabilities of the NMIs for a particular measurement or calibration service, coupled with satisfactory performance on a key comparison of the same measurement or standard by each of the NMIs.
Laboratory accreditation MRAs are established among accreditation bodies, domestically and internationally, for the purpose of recognizing the equivalence of their respective accreditation systems. To be invited to sign an MRA, each accreditation body must undergo an evaluation by its peers to determine its capability and competence to meet documented requirements for the operation of such bodies. Included is the ability of the accreditation body to accredit laboratories to the requirements of the internationally recognized standard ISO/IEC 17025 . The purpose of these MRAs is to provide the means by which users of calibration and testing services can have confidence in the calibration and test reports issued by a laboratory that has been accredited by any of the accreditation body signatories to the MRA. The goals are to reduce or eliminate redundant audits by having one evaluation of a laboratory satisfy the needs of the user community and to have the results of calibrations or tests accepted across borders. By signing the arrangement, each signatory is obligated to promote the acceptance of the results of calibrations or tests conducted by the accredited laboratories of any other signatory to the MRA as being technically equivalent to its own. This does not mean that signatory accreditation bodies accept or promote the acceptance of claims of traceability to sources other than NIST as being equal to traceability to standards maintained by NIST. All calibration and test reports must declare the source of traceability and it is the responsibility of the user to determine which source is suitable for its needs. Other tools, such as the CIPM MRA and the databases resulting from this MRA, are meant to assist the users in making this decision. (See Questions II.E.1 and II.E.2 above.)
I.E.4 Because NIST’s National Voluntary Laboratory Accreditation Program (NVLAP) is a signatory to multiple MRAs with other accreditation bodies, does that mean NIST stands behind claims of traceability made by any laboratory accredited by any other MRA signatory?
As previously stated, laboratory accreditation, whether conducted by NVLAP or any other recognized accreditation body, is a finding of a laboratory’s competence and capability to provide technically sound and appropriate measurement services within their scope of accreditation. As a signatory to MRAs operated under the auspices of the Asia-Pacific Laboratory Accreditation Cooperation (APLAC) and the International Laboratory Accreditation Cooperation (ILAC), NVLAP promotes international acceptance of test, calibration and inspection reports and other documents issued by laboratories and inspection bodies accredited by signatories to the MRAs.All calibration and test reports must declare the source of traceability and it is the responsibility of the user to determine which source is suitable for its needs.
There are about 2 million workers in the United States whose occupational exposure to ionizing radiation is monitored on a continuing basis. These populations include nuclear power plant workers, radiological personnel in health care, and Department of Defense civilian and military personnel associated with submarines, aircraft carriers, nuclear weapons or other radiological activities. The accuracy of the millions of individual measurements depends on instrument calibrations that are traceable to NIST primary standards for ionizing radiations (primarily calibrations for electrons, x-rays, gamma rays and neutrons). The organizations and communities involved include the NIST Physics Laboratory, the NIST National Voluntary Laboratory Accreditation Program (NVLAP), Battelle Pacific Northwest National Laboratory, the Nuclear Regulatory Commission, and the American National Standards Institute (ANSI) Subcommittee N13.11. (Reference )
There are approximately 37,000 nuclear medicine procedures performed daily in U.S. hospitals and clinics in which radioactively labeled drugs are administered to patients. These are mainly used in the diagnosis of cancer, cardiovascular disease and neurological disorders ranging from stroke patients to Alzheimer’s disease. In addition to the diagnostic procedures, there are over 100,000 therapeutic nuclear medicine procedures per year - mainly iodine-131 for thyroid cancer and hyperthyroidism, and new agents for bone palliation for terminal cancer patients. The accuracy of each of these pharmacological administrations depends on transfer instruments used in the manufacturing processes that are traceable to NIST primary standards for radioactivity. The organizations involved include the pharmaceutical manufacturers of North America, under the auspices of the Nuclear Energy Institute, the U.S. Food and Drug Administration, the NIST Physics Laboratory and the NIST Standard Reference Materials Program. (Reference )
There are over 100 operating nuclear power stations in the U.S. and numerous Department of Energy (DoE) and Department of Defense (DoD) sites that must be monitored for release of radioactive gaseous and liquid effluents. The continuing accuracy of these measurements is a concern to the DOE, DOD and to the Nuclear Regulatory Commission and the Environmental Protection Agency. Radioanalytical instrumentation must be calibrated using radioactive sources that are traceable to the primary radioactivity standards at NIST. Organizations involved include the source manufacturers, the Nuclear Energy Institute, the NIST Physics Laboratory, the NIST Calibration Program, other government agencies and the American National Standards Institute Subcommittee ANSI N42.2. (Reference )
NIST, in partnership with the Environmental Protection Agency (EPA) and 10 specialty gas companies established the NIST Traceable Reference Material (NTRM) Program for gas mixture standards as a means for providing end users with the large volumes of NIST-traceable gas mixture standards needed to implement the "Emissions Trading" provision of the 1990 Clean Air Act. In general, an NTRM is a reference material produced and distributed by a commercial supplier with a well-defined traceability linkage to NIST. This linkage is established via criteria and protocols defined by NIST that are tailored to meet the needs of the metrological community to be served. The production and value-assignment protocols required are based on NIST experience in the production and certification of its own gas mixture SRMs. The integrity of the NTRMs produced is assured by NIST through an active internal quality assurance program that includes NIST analysis of at least 10 % of each NTRM batch and NIST value-assignment of each batch based on NIST and client company measurements .
Ion-implanted standards of known dose are needed to calibrate secondary ion responses for Secondary Ionization Mass Spectrometry (SIMS) in the semiconductor industry. SIMS is relied upon to measure the concentrations and depth profiles of key dopants in silicon, but SIMS measurement results are matrix dependent. A reference material is needed for each element and matrix combination and the comparability of SIMSresults when calibrated with reference materials from different sources is not sufficient to meet the needs of the semiconductor community. An accuracy-based transfer standard from NIST enables the industry to transfer technology from one manufacturing site to another, compare experimental data with theoretical process models, and provide the basis for international comparability via ISO (International Organization for Standardization) standards.
A NIST reference method for arsenic in silicon based on Neutron Activation Analysis was developed and critically evaluated. Twenty-nine sources of uncertainty were identified and quantified, of which seven accounted for 98 % of the total uncertainty. This reference technology was transferred to the semiconductor community through certification of SRM 2134, Ion-Implanted Arsenic in Silicon, which has an expanded uncertainty of 0.38 % . The 1999 International Technology Roadmap for Semiconductors (ITRS) calls for improvement in dopant profile concentration measurements from ± 5 % in 1999 to ± 2 % in 2008. These values are to be accomplished with "low systematic error" as well. SRM 2134 has met these requirements for arsenic since 2001.
The SI defines temperature on the Kelvin Thermodynamic Scale. In practice, temperature is measured on the more easily realized International Temperature Scale of 1990 (ITS-90), which is a close approximation to the Kelvin scale. As custodian of the ITS-90 scale, NIST provides to its customers:
An example of traceability to NIST temperature standards is the Measurement Assurance Program (MAP), as implemented with Standard Platinum Resistance Thermometers (SPRTs) in the range - 190° C to 660° C. In a MAP, NIST sends to a customer who realizes the ITS-90 or an approximation to the ITS-90 a set of three SPRTs that have previously been calibrated by NIST on the ITS-90. The customer calibrates the set of SPRTs and then returns the SPRTs to NIST for a final calibration. NIST analyzes the raw data, uncertainty statements, methods of data analysis, methods of realization of the ITS-90, calibration report results and format. A full descriptive report of this analysis is sent to the customer with suggestions for improvement and a quantitative statement of the present level of agreement of the customer calibrations with the NIST calibrations. A MAP is a quantitative test of the customer’s ability to calibrate SPRTs and of the validity of the claimed uncertainties of the calibrations. When conducted at regular intervals, a MAP supports the customer’s claim of continuous traceability to NIST at a specified uncertainty [13-14].
The international standard for time and frequency metrology is the Coordinated Universal Time Scale (UTC) maintained by the BIPM in Paris, France. Traceability of time and frequency standards is required for the calibration and testing of devices from simple mechanical timers to state-of-the-art atomic oscillators. NIST maintains a real time version of the UTC and offers services that provide high accuracy traceability. The NIST Frequency Measurement and Analysis Service (FMAS) allows users to lease a complete measurement system from NIST. The FMAS includes a GPS receiver, all necessary measurement hardware, and a data line back to NIST. All measurements are made automatically, and are traceable to NIST at an uncertainty of 2 x 10-13 per day. NIST oversees the entire measurement process, and is responsible for both measurements and uncertainty analysis. See http://www.nist.gov/physlab/div847/grp40/fmas.cfm for a complete description. (Reference )
calibration – set of operations that establish, under specified conditions, the relationship between values of quantities indicated by a measuring instrument or measuring system, or values represented by a material measure or reference material, and the corresponding values realized by standards. (International vocabulary of metrology - Basic and general concepts and associated terms Reference , definition 2.39)
calibration and measurement certificates – the result of a calibration may be recorded in a document, sometimes called a calibration certificate or a calibration report. Also can refer to a document accompanying a certified reference material (such as a NIST SRM) stating one or more property values and their uncertainties, and confirming that the necessary procedures have been carried out to ensure their validity and traceability [1, 16]. See also 
certified reference material (CRM)– A reference material (RM) characterized by a metrologically valid procedure for one or more specified properties, accompanied by a certificate that provides the value of the specified property, its associated uncertainty, and a statement of metrological traceability. The concept of value includes qualitative attributes such as identity or sequence. Uncertainties for such attributes may be expressed as probabilities 
internal measurement assurance program – program of sufficient complexity, within an organization, to provide credibility to the measurement uncertainty and measurement result for which traceability is to be established. An internal measurement assurance program usually involves monitoring the performance (e.g., stability, reproducibility) of the instrument, standard, or measurement system, before and after it is characterized, calibrated, or used to obtain the traceable measurement result.
laboratory accreditation – procedure by which an authoritative body gives formal recognition that a laboratory is competent to carry out specific tasks. Accreditation does not itself qualify the laboratory to approve any particular product. However, accreditation may be relevant to approval and certification authorities when they decide whether or not to accept data produced by a given laboratory in connection with their own activities .
measurement result – According to the VIM: set of quantity values being attributed to a measurand together with any other available relevant information, generally expressed as a single measured quantity value and a measurement uncertainty. The concept of traceability covers both measurement results of quantity values and of nominal property values such as chemical identity and sequence (Reference , definition 2.9).
measurement uncertainty – Here meaning uncertainty of measurement that: (1) fulfills the VIM definition as the parameter, associated with the result of a measurement, that characterizes the dispersion of values that could reasonably be attributed to the measurand; (2) is evaluated and expressed according to the general rules given in the ISO Guide to the Expression of Uncertainty in Measurement (or other sound and accepted method); and (3) is explicitly set forth in supporting documentation.
national or international standards – here meaning measurement standards. Standards (national) recognized by a national decision to serve, in a country, as the basis for assigning values to other standards of the quantity concerned; standards (international) recognized by an international agreement to serve internationally as the basis for assigning values to other standards of the quantity concerned .
NIST Traceable Reference Material (NTRM) – a reference material produced by a commercial supplier with a well-defined traceability to NIST established via criteria and protocols defined and documented by NIST and tailored to meet the needs of the metrological community to be served .
official NIST program or collaboration – Here meaning a NIST program or collaboration, officially approved by NIST management, in which NIST formally assures or certifies traceability of the results of measurements other than those that NIST itself provides.
organizations that have authority and responsibility for variously defining, specifying, assuring, or certifying traceability – Here meaning any regulatory agency, standards developing organization, accreditation body, trade association or the like, which, by law or mutual agreement, is assigned or takes on authority and responsibility for some aspect of defining, specifying, assuring, or certifying traceability.
reference material (RM) – Material, sufficiently homogeneous and stable with respect to one or more specified properties, which has been established to be fit for its intended use in a measurement process. RM is a generic term, and properties can be quantitative or qualitative, e.g., identity of substances or species .
specified reference – Here taken to mean "specified reference measurement standard", where: (1) specified here means explicitly set forth in supporting documentation, and (2) a reference measurement standard, which, according to the VIM, is a measurement standard, generally having the highest metrological quality available at a given location or in a given organization, from which measurements there are derived. A national measurement standard is a standard recognized by a national authority to serve in a state or economy as the basis for assigning quantity or nominal property values to other standards of the quantity or kind concerned. An international measurement standard is a standard recognized by signatories to an international agreement and intended to serve worldwide.
Standard Reference Data (SRD) – quantitative information, related to a measurable physical or chemical property of a substance or system of substances of known composition and structure, which is critically evaluated as to its reliability (Standard Reference Data Act, 15 U.S.C. 290 Sec. 2(a)).
Standard Reference Material (SRM) – certified reference materials (CRMs) issued under the NIST trademark. NIST Standard Reference Materials are characterized using state-of-the-art measurement methods and/or technologies for the determination of chemical composition and/or physical properties. The property values of an SRM are certified by a process that establishes traceability to an accurate realization of the unit in which the property values are expressed or to a national standard defined de facto by a conventionally stated method. Each certified value is accompanied by an uncertainty at a stated level of confidence. SRMs are issued by NIST with a certificate that reports the results of the characterization and indicates the intended use of the material.
stated uncertainties – uncertainty of measurement that: (1) fulfills the International vocabulary of metrology - Basic and general concepts and associated terms  definition as the parameter, associated with the result of a measurement, that characterizes the dispersion of values that could reasonably be attributed to the measurand; (2) is evaluated and expressed according to the general rules given in the ISO Guide to the Expression of Uncertainty in Measurement ; and (3) is explicitly set forth in supporting documentation
unbroken chain of calibrations – Here taken to mean the complete, explicitly described, and documented series of calibrations that successively link the value and uncertainty of a result of measurement with the values and uncertainties of each of the intermediate reference standards and the highest reference standard to which traceability for the result of measurement is claimed. A calibration is the operation that, under specified conditions, in a first step, establishes a relation between the quantity values with measurement uncertainties provided by measurement standards and corresponding indications with associated measurement uncertainties and, in a second step, uses this information to establish a relation for obtaining a measurement result from an indication.
unbroken chain of comparisons – complete, explicitly described, and documented series of comparisons that successively link the value and uncertainty of the result of a measurement with the values and uncertainties of each of the intermediate reference standards and the highest reference standard to which traceability for the result of measurement is claimed.
user of result – That is, the user of the result of a measurement; the individual or organization that receives for use the result of measurement for which metrological traceability is being asserted.
A high-level checklist for traceability through calibration is as follows:
Element #1 (performed at customer facility, responsibility of customer)
Element #2 (performed at reference laboratory, responsibility of reference laboratory)
Element #3 (performed at customer facility, responsibility of customer)
Element #4 (performed at customer facility, responsibility of customer)
The Elements in this checklist are depicted schematically in the figure below (see Reference 1):