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Synchrotron Science Group

The Synchrotron Science Group advances X-ray measurements of materials through NIST developed and operated beamlines at the National Synchrotron Light Source II (NSLS II). Measurements are developed to support collaborative projects across NIST and the NSLS II user community. The group advances this mission through a decades long strategic partnership with the Department of Energy and Brookhaven National Laboratory.

Central to the multi-decade NIST BNL strategic partnership in synchrotron technology, the Synchrotron Science Group develops state of-the-art synchrotron X-ray measurement technology around a core-competency in X-ray absorbance spectroscopy. The SSG develops instrumentation, methods, and analytical tools, to enable measurements of structure not attainable by other methods. Stationed at the National Synchrotron Light Source II (NSLS-II) at Brookhaven National Laboratory, the group provides timely access to X-ray facilities to support both NIST priority programs as well as the broader scientific community through the NSLS-II General User Program. Working closely with other units across NIST, new advances in instrumentation are connected to a broad range of NIST stakeholders. Primary examples are the development of the Resonant Soft X-ray Scattering instrument in close collaboration with the Materials Science and Engineering Division and the development of microcalorimeter detector technologies with the NIST Quantum Sensing Division. Outside partnerships have also been key to the technology transfer strategy, with a co-developed and operated end station in X-ray Diffraction with IBM, and imaging capabilities developed through two Small Business Innovation and Research Awards. Additional collaborations with industry such as Dow Chemical and SEMATECH are complemented with ongoing development with other agencies such as the Air Force Research Laboratory and Sandia National Laboratory. The group has been a world leader in the development of adsorbtion spectroscopy software, with world-wide adoption and high demand for online courses and workshops. The group features three main thrusts that all build on the core competency in absorbance spectrometry: adsorbance spectrometers, hyperspectral imaging, and resonant scattering and diffraction.

News and Updates

Projects and Programs

Synchrotron X-ray Absorbance Spectroscopy

Ongoing
The Absorbance Spectroscopy effort seeks to develop measurements that provide details of the local chemical, electronic, and physical structure in advanced materials. Spectrometer technology is developed as part of the NIST BNL partnership at the National Synchrotron Light Source II in Upton, NY

Synchrotron X-ray Spectroscopic Imaging

Ongoing
Building off technologies and expertise developed in the Synchrotron X-ray Absorption Spectroscopy project, the Spectroscopic Imaging effort seeks to develop measurements that provide spatial mapping of the local chemical, electronic, and physical structure in advanced materials. Technology is

Synchrotron Resonant Scattering and Diffraction

Ongoing
The Resonant Scattering and Diffraction effort seeks to develop measurements that provide spatial correlations in chemical, electronic, and physical structure in advanced materials. Scattering technology is developed as part of the NIST BNL partnership at the National Synchrotron Light Source II in

Publications

Observation of a promethium complex in solution

Author(s)
Bruce D. Ravel, Darren Driscoll, Frankie White, SUBHAMAY PRAMANIK, Jeffrey Einkauf, Dmytro Bykov, Santanu Roy, Richard Mayes, Laetitia Delmau, Samantha Schrell, Thomas Dyke, April Miller, Matt Silveira, Silveira2 van Cleve, Roy Copping, Sandra Davern, Santa Jansone-Popova, Ilja Popovs, Alexander Ivanov
Lanthanide rare earth metals are ubiquitous in modern technologies, but we know little about chemistry of the 61st element, promethium (Pm), a lanthanide which

Tools and Instruments

X-ray Absorption Fine Structure (XAFS)

The XAFS station uses a tunable, monochromatic, and moderately high energy X-ray beam (4.5 keV to 23.5 keV) for X-ray absorption spectroscopy measurements. The

Awards

Contacts

Group Leader

Office Manager