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Angela R. Hight Walker (Fed)

Dr. Angela R. Hight Walker, a senior scientist at NIST, is renowned for pioneering optical spectroscopies, both Raman and Photoluminescence (PL) to characterize quantum materials. A current focus area is using optical signatures to study magnetic order. Over three decades, she has led research on low-dimensional materials, contributing nearly 200 publications at the intersection of physics, chemistry, and materials science. A Fellow of the American Physical Society (APS), American Association for the Advancement of Science (AAAS), and Sigma Xi, she also plays a key role in international nanotechnology and Raman standardization efforts as a technical expert and scientific diplomate.

An issue of great importance to Dr. Hight Walker is encouraging the young to participate in science. Through on and offsite demonstrations, lectures, and conferences she activity engages in promoting the excitement of science. Recruiting, encouraging and mentoring high school and undergraduate students and postdoctoral researchers is a passion of Angela’s, having hosted over 50 during her tenure at NIST.

Research details

Novel Instrumentation for Quantum Material Characterization: 
Combined Magneto-Optical Magneto-Transport

Raman spectroscopy, imaging, and mapping are powerful non-contact, non-destructive optical probes of quasiparticles and fundamental physics in graphene and other related two-dimensional (2D) materials, including layered, quantum materials. An amazing amount of information can be quantified from the Raman spectra, including layer thickness, disorder, edge and grain boundaries, doping, strain, thermal conductivity, magnetic ordering, and features from unique excitations such as magnons and charge density waves can be observed. Most interestingly for quantum materials is that Raman efficiently probes the evolution of the electronic structure and the electron-phonon, spin-phonon, and magnon-phonon interactions as a function of laser energy and polarization, temperature, and applied magnetic field. Our unique magneto-Raman spectroscopic capabilities enable spatially-resolved, diffraction-limited optical measurements (either Raman or photoluminescence) while simultaneously supporting electrical magneto-transport measurements including quantum Hall.

Upcoming Invited Talks in 2025

Selected Publications

Surface-Enhanced Raman Spectroscopy via Gold Nanostars

Author(s)
Emren Nalbant-Esenturk, Angela R. Hight Walker
Anisotropic metallic nanoparticles have unique optical properties, which lend them to applications such as Surface Enhanced Raman Spectroscopy (SERS). Branched

Publications

Reproducible graphene synthesis by oxygen-free chemical vapour deposition

Author(s)
Jacob Amontree, Xingzhou Yan, Christopher DiMarco, Pierre Levesque, Tehseen Adel, Jordan Pack, Madisen Holbrook, Christian Cupo, Zhiying Wang, Dihao Sun, Adam Biacchi, Charlezetta Stokes, Kenji Watanabe, Takashi Taniguchi, Cory Dean, Angela R. Hight Walker, Katayun Barmak, Richard Martel, James Hone
The demonstration of large-scale graphene synthesis on Cu by chemical vapor deposition (CVD) has led to enormous interest worldwide over the past 14 years. The

Ring-exchange interaction effects on magnons in the Dirac magnet CoTiO3

Author(s)
Yufei Li, Thuc Mai, Mohammed Karaki, Evan Jasper, Kevin Garrity, Chase Lyon, Daniel Shaw, Timmothy DeLazzer, Adam Biacchi, Rebecca Dally, Daniel Heligman, Jared Gdanski, Tehseen Adel, Maria Munoz, Alex Giovannone, Amit Pawbake, Clément Faugeras, Jeffrey Simpson, Kate Ross, Nandini Trivedi, Yuanming Lu, Angela R. Hight Walker, Rolando Valdes Aguilar
In magnetically ordered materials with localized electrons, it has been known for a long time [1–3] that the fundamental interactions are due to exchange of

Patents (2018-Present)

pic for 10,858,256

Redox Sorting of Carbon Nanotubes

NIST Inventors
Angela R. Hight Walker and Ming Zheng
A method of separating and extracting carbon nanotubes, the method includes introducing the carbon nanotubes into a two-phase system that includes a first component and a second component, the first component being different from the second component. The method includes introducing a chemical agent
Created October 9, 2019, Updated February 5, 2025