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Search Publications by: Lane C. Sander (Fed)

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Displaying 76 - 100 of 447

Sample Concentration and Processing

January 12, 2017
Author(s)
Lane C. Sander
Sample Concentration and Processing Sample concentration is a common step in sample preparation prior to analysis that is performed to increase method sensitivity or to exchange solvent environment. Sample concentration can be thought of as a separation

Soxhlet Extractions

January 12, 2017
Author(s)
Lane C. Sander
Soxhlet extraction is one of several sample preparation methods that can be used to transfer targeted analytes from a sample matrix into a solvent, to permit subsequent analysis. With Soxhlet extraction, samples are repeatedly extracted with solvent

Troubleshooting Liquid Chromatographic Instrumentation and Methods

January 12, 2017
Author(s)
Lane C. Sander
The ability to assess analytical performance is a fundamental component of measurement science. Ultimately, measurement quality depends on the proper function of instrumentation in combination with appropriate methods. Evidence of proper function is

Use of Analytical Balances

January 12, 2017
Author(s)
Lane C. Sander
The determination of mass is a fundamental component in quantitative analysis, and weighing accuracy is an important factor for most applications. This presentation will highlight the use of different types of analytical balances and will demonstrate

Volumetric Transfer of Liquids

January 12, 2017
Author(s)
Lane C. Sander
Although volumetric measurements are usually less accurate than gravimetric based measurements, volumetric measurements are still in common use due to the convenience, and often higher throughput, that may be afforded by automatic pipettes. Analysts should

What is Chromatography All About?

January 12, 2017
Author(s)
Lane C. Sander
Chromatography is an example of a process by which a mixture is separated into at least two fractions with different compositions. Other separation methods exist, such as distillation, recrystallization, and extraction. Chromatography is used to analyze

Retention behavior of alkyl-substituted polycyclic aromatic sulfur heterocycle isomers in gas chromatography on stationary phases of different selectivity

January 10, 2017
Author(s)
Walter B. Wilson, Lane C. Sander, Jorge O. Ona Ruales, Stephanie Mossner, Leonard M. Sidisky, Milton Lee, Stephen A. Wise
Retention indices for 10 sets of alkyl-substituted polycyclic aromatic sulfur heterocycles (PASHs) isomers (total of 80 PASHs) were determined using gas chromatography with three different stationary phases: a 50% phenyl phase, a 50% liquid crystalline

Retention behavior of isomeric polycyclic aromatic sulfur heterocycles in gas chromatography on stationary phases of different selectivity

January 10, 2017
Author(s)
Walter B. Wilson, Lane C. Sander, Jorge O. Ona Ruales, Leonard M. Sidisky, Milton Lee, Stephen A. Wise
Retention indices for 70 polycyclic aromatic sulfur heterocycles (PASHs) were determined using gas chromatography with three different stationary phases: a 50% phenyl phase, a 50% liquid crystalline dimethylpolysiloxane (LC-DMPS) phase, and an ionic liquid

Summary of NIST/SIM Chemical Metrology Working Group Training Opportunity: Isotope Dilution-Mass Spectrometry Clinical Measurement Course

December 22, 2016
Author(s)
Jeanita Pritchett, Katrice A. Lippa, Mary Bedner, Carolyn Q. Burdette, Johanna Camara, Brian E. Lang, Michael A. Nelson, Lane C. Sander, Lorna T. Sniegoski
The one week NIST-SIM chemical metrology training opportunity was designed to provide SIM NMI/DI laboratory personnel with in-depth classroom and hands-on laboratory experience for the implementation of isotope dilution/mass spectrometry (ID/MS) methods in

Liquid Chromatography with Absorbance Detection and with Isotope-Dilution Mass Spectrometry for Determination of Isoflavones in Soy Standard Reference Materials

November 10, 2016
Author(s)
Melissa M. Phillips, Mary Bedner, Manuela Reitz, Carolyn Q. Burdette, Michael A. Nelson, James H. Yen, Lane C. Sander, Catherine A. Rimmer
Two independent analytical approaches, based on liquid chromatography with absorbance detection and liquid chromatography with mass spectrometric detection, have been developed for determination of isoflavones in soy materials. These two methods yield

The influence of the aromatic character in the gas chromatography elution order: the case of polycyclic aromatic hydrocarbons

November 8, 2016
Author(s)
Jorge O. Ona Ruales, Walter B. Wilson, Federica Nalin, Lane C. Sander, Patricia Schubert, Stephen A. Wise
A link between the aromatic character of polycyclic aromatic hydrocarbons (PAHs) and gas chromatography (GC) elution order in columns with a polysiloxane backbone in the stationary phase is reported for the first time. The aromatic character was calculated