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Search Publications by: Angela R. Hight Walker (Fed)

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Displaying 101 - 125 of 254

State of the Art Raman Techniques for Biological Applications

July 1, 2014
Author(s)
Angela R. Hight Walker, Alasdair Rae, Rainer Stosch, Petr Klapetek, Debdulal Roy
Raman spectroscopy is a powerful tool for the elucidation of qualitative and quantitative information from biological systems and has huge potential in areas such as biotechnologies, drug discovery, agro-chemical research and clinical diagnostics. This

Tearing and scrolling of transferred graphene

April 29, 2014
Author(s)
Guangjun Cheng, Brent A. Sperling, James E. Maslar, Curt A. Richter, Angela R. Hight Walker
We present an investigation on tearing and scrolling of the transferred graphene on a Si/SiO2 substrate. Graphene grown by chemical vapor deposition (CVD) is transferred onto a Si/SiO2 substrate using a wet polymer-mediated process. Upon the removal of

Highly reproducible and reliable metal/graphene contact by UV-Ozone treatment

March 17, 2014
Author(s)
Wei Li, Christina A. Hacker, Guangjun Cheng, Angela R. Hight Walker, Curt A. Richter, David J. Gundlach, Yiran Liang, boyuan Tian, Xuelei Liang, Lianmao Peng
Resist residue from the device fabrication process is a significant source of contamination at the metal/graphene contact interface. Ultraviolet Ozone (UVO) treatment is proven here, by X-ray photoelectron spectroscopy (XPS) and Raman measurement, to be an

Isolation of Specific Small Diameter Single-Wall Carbon Nanotube Species via Aqueous Two-Phase Extraction

January 21, 2014
Author(s)
Jeffrey A. Fagan, Constantine Y. Khripin, Carlos A. Silvera Batista, Jeffrey R. Simpson, Angela R. Hight Walker, Ming Zheng
Aqueous two-phase extraction (ATPE) is demonstrated to enable isolation of multiple semiconducting and metallic single-wall carbon nanotube species from a small diameter synthetic mixture. Separation by ATPE is rapid and robust, with remarkable tunability

Thermal Conductivity of Monolayer MoS2 Obtained from Temperature-Dependent Raman Spectroscopy

December 30, 2013
Author(s)
Rusen Yan, Jeffrey R. Simpson, Simone Bertolazzi, Jacopo Brivio, Michael Watson, Xufei Wu, Andras Kis, Tengfei Luo, Angela R. Hight Walker, Huili G. Xing
Atomically thin molybdenum disulphide (MoS2) is emerging as a potential alternative to graphene due to presence of bandgap, which is particularly advantageous to optoelectronic applications. The temperature-dependent Raman spectra of exfoliated monolayer

Analyzing Surfactant Structures on Length and Chirality Resolved (6,5) Single-Wall Carbon Nanotubes by Analytical Ultracentrifugation

March 26, 2013
Author(s)
Jeffrey A. Fagan, Ming Zheng, Jeffrey R. Simpson, Vinayak Rastogi, Constantine Y. Khripin, Carlos A. Silvera Batista, Angela R. Hight Walker
The structure and density of the bound interfacial surfactant layer and associated hydration shell were investigated using analytical ultracentrifugation for length and chirality purified (6,5) single-wall carbon nanotubes (SWCNTs) in three different bile

Determination of graphene work function and graphene-insulator-semiconductor band alignment by internal photoemission spectroscopy

July 11, 2012
Author(s)
Rusen Yan, Qin Zhang, Wei Li, Irene G. Calizo, Tian T. Shen, Curt A. Richter, Angela R. Hight Walker, Xuelei X. Liang, David J. Gundlach, Nhan Van Nguyen, Huili G. Xing, Alan Seabaugh
We determined the band alignment of a graphene-oxide-silicon structure using internal photoemission spectroscopy. From the flatband voltage and Dirac voltage we infer a 4.3  10e11 cm-2 negative extrinsic charge present on the graphene surface. Also, we

Characteristics of Graphene for Quantized Hall Effect Measurements

June 1, 2012
Author(s)
Randolph E. Elmquist, Mariano A. Real, Irene G. Calizo, Brian G. Bush, Tian T. Shen, Nikolai N. Klimov, David B. Newell, Angela R. Hight Walker, Randall M. Feenstra
This paper describes concepts and measurement techniques necessary for characterization of graphene in the development of graphene-based quantized Hall effect (QHE) devices and resistance standards. We briefly contrast the properties of graphene produced

Relationship between Length and Surface-Enhanced Raman Spectroscopy signal Strength in Metal Nanoparticle Chains: Idea Models versus Nanofabrication

January 18, 2012
Author(s)
Angela R. Hight Walker, K. Stec, Shunpig Zhang, Hongxing Xu, Rene Lopez
We have employed capillary force deposition on ion beam patterned substrates to fabricate chains of 60nm gold nanospheres ranging in length from 1 to 9 nanoparticles. Measurements of the surface-averaged SERS enhancement factor strength for these chains

Towards clean and crackless transfer of graphene

January 2, 2012
Author(s)
Xuelei X. Liang, Brent A. Sperling, Irene G. Calizo, Guangjun Cheng, Christina Hacker, Qin Zhang, Yaw S. Obeng, Kai Yan, Hailin Peng, Qiliang Li, Xiaoxiao Zhu, Hui Yuan, Angela R. Hight Walker, Zhongfan Liu, Lianmao Peng, Curt A. Richter
We present the results of a thorough study of wet chemical methods for transferring chemical vapor deposition grown graphene from the metal growth substrate to a device compatible substrate. Based on these results, we have developed a "modified RCA clean"

A Highly Practical Route for Large-Area, Single Layer Graphene from Liquid Carbon Sources such as Benzene and Methanol

October 28, 2011
Author(s)
Gadipelli Srinivas, Irene G. Calizo, Jamie Ford, Guangjun Cheng, Angela R. Hight Walker, Taner N. Yildirim
Through a detailed systematic study, we determined the parameters critical for high-quality, single-layer graphene formation and developed a straightforward synthesis that requires no explosive hydrogen or methane gas flow. The synthesis is further

Separation of Empty and Water-Filled Single-Wall Carbon Nanotubes

April 11, 2011
Author(s)
Jeffrey A. Fagan, Jeffrey R. Simpson, JiYeon Huh, Jeffrey Blackburn, Larsen A. Brian, Josh M. Holt, Angela R. Hight Walker
The separation of empty and water-filled laser ablation and electric arc synthesized nanotubes is reported. Centrifugation of these large-diameter nanotubes dispersed with sodium deoxycholate using specific conditions produces isolated bands of empty and

Evolution of Microscopic Localization in Graphene in a Magnetic Field: From Scattering Resonances to Quantum Dots.

January 9, 2011
Author(s)
Suyong S. Jung, Gregory M. Rutter, Nikolai Klimov, David B. Newell, Irene G. Calizo, Angela R. Hight Walker, Nikolai Zhitenev, Joseph A. Stroscio
Graphene is a unique material displaying high-mobility transport in monolayer-thin films. However, its properties are strongly dependent on interactions with substrates, local charges and environment. Scanned probe microscopies can be used to locally probe