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Search Publications by: Jason Killgore (Fed)

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Displaying 1 - 25 of 77

Additive Manufacturing of Highly Entangled Polymer Networks

August 1, 2024
Author(s)
Abhishek Dhand, Matthew Davidson, Hannah Zlotnick, Thomas Kolibaba, Jason Killgore, Jason Burdick
Incorporation of polymer chain entanglements within a single network can synergistically improve stiffness and toughness, yet attaining such dense entanglements through vat photopolymerization additive manufacturing (e.g., digital light processing, DLP)

Effects of hydrogen on the evolution of 4130 steel microstructure as a result of tensile loading

July 12, 2024
Author(s)
Zack Buck, May Ling Martin, Damian Lauria, Jason Killgore, Peter Bradley, Yan Chen, Ke An, Matthew Connolly
Neutron diffraction and Scanning Kelvin Probe Force Microscopy (SKPFM) were used to study the evolution of lattice strain, dislocation density, and phase partitioning of a ferrite/martensite pressure vessel steel (AISI 4130) that resulted from tensile

Influence of Spectral Bandwidth on the Working Curve in Vat Photopolymerization

April 29, 2024
Author(s)
Benjamin Caplins, Thomas Kolibaba, Uwe Arp, C Cameron Miller, Yuqin Zong, Dianne L. Poster, Callie Higgins, Jason Killgore
In vat photopolymerization, 3-dimensional parts are fabricated by using patterned light to spatially cure a liquid resin. One of the foundational measurements for vat photopolymerization is known as the working curve whereby the depth (i.e. thickness) of

Results of an Interlaboratory Study on the Working Curve in Vat Photopolymerization

March 18, 2024
Author(s)
Thomas Kolibaba, Jason Killgore, Benjamin Caplins, Callie Higgins, Uwe Arp, C Cameron Miller, Yuqin Zong, Dianne L. Poster
The working curve informs resin properties and print parameters for stereolithography, digital light processing, and other photopolymer additive manufacturing (PAM) technologies. First demonstrated in 1992, the working curve measurement of cure depth vs

Polybutadiene Click Chemistry: A Rapid and Direct Method for Vat Photopolymerization

October 10, 2023
Author(s)
Levi Moore, Van Michael Saludo, Oliver Grasdal, Kayleen Smith, Thomas Kolibaba, Jason Killgore, Jacob Marcischak, Jeremy Snyder, Gregory Yandek, Kamran Ghiassi
Thiol-ene click chemistry was utilized to crosslink unmodified commercial liquid polybutadiene, and complex geometries were printed using vat photopolymerization. Polybutadiene contains reactive moieties as a result of its production process, and were used

Effects of mechanical deformation on dislocation density and phase partitioning in 4130 steel

August 22, 2023
Author(s)
Zack Buck, Matthew Connolly, May Ling Martin, Damian Lauria, Jason Killgore, Peter Bradley, Yan Chen, Ke An, Andrew Slifka
Interrupted tensile tests were performed on an AISI 4130 pressure vessel steel and investigated by neutron diffraction and scanning microscopy techniques. Analysis of the neutron diffraction patterns reveal a partitioning of ferrite and martensite phases

A Data-Driven Approach to Complex Voxel Predictions in Grayscale Digital Light Processing Additive Manufacturing Using U-nets and Generative Adversarial Networks

July 6, 2023
Author(s)
Jason Killgore, Thomas Kolibaba, Benjamin Caplins, Callie Higgins, Jake Rezac
Machine learning models such as U-nets like the pix2pix conditional generative adversarial network (cGAN) are shown to predict 3D printed voxel geometry in digital light processing (DLP) additive manufacturing. The models are trained on microscopic voxel

Influence of Fluorescent Dopants on the Vat Photopolymerization of Acrylate-based Plastic Scintillators

July 3, 2023
Author(s)
Thomas Kolibaba, Jason Killgore, Caleb Chandler, Dominique Porcincula, Michael Ford, Benjamin Fein-Ashley, Jason Brodsky, Alan Sellinger
Plastic scintillators, a class of solid-state materials used for radiation detection, were additively manufactured with vat photopolymerization. The photopolymer resins consisted of a primary dopant and a secondary dopant dissolved in a bisphenol A

Synergistic Fire Resistance of Nanobrick-wall Coated 3D Printed Photopolymer Lattices

March 16, 2023
Author(s)
Thomas Kolibaba, Callie Higgins, Zack Buck, Dash Weeks, Jason Killgore
Photopolymer additive manufacturing has become the subject of widespread interest in recent years due to its capacity to enable fabrication of difficult geometries that are impossible to build with traditional modes of manufacturing. The flammability of

Sustainable Additive Manufacturing of Polyelectrolyte Photopolymer Complexes

January 29, 2023
Author(s)
Thomas Kolibaba, Jason Killgore, Callie Higgins
Polyelectrolyte complexes (PECs), assemblies of oppositely charged polymers with powerful properties and wide-ranging applications, are currently not melt-processable via any conventional means and have been limited commercially to applications only as

Characterizing light engine uniformity and its influence on LCD-based vat photopolymerization printing

December 27, 2022
Author(s)
Benjamin Caplins, Callie Higgins, Thomas Kolibaba, Uwe Arp, C Cameron Miller, Dianne L. Poster, Clarence Zarobila, Yuqin Zong, Jason Killgore
Vat photopolymerization (VP) is a rapidly growing category of additive manufacturing. As VP methods mature the expectation is that the quality of printed parts will be highly reproducible. At present, detailed characterization of the light engines used in

Degradation of CVD-Grown MoS2 Subjected to DC Electrical Stress

September 16, 2022
Author(s)
Elisabeth Mansfield, David Goggin, Jason Killgore, Taylor Aubry
Devices containing transition metal dichalcogenides are being investigated for next generation electronics. Understanding material properties under typical use conditions is important for longevity and effectiveness of these devices. In this study, CVD

In situ absorption synchrotron measurements, predictive modeling, microstructural analysis, and scanning probe measurements of laser melted Ti-6Al-4V single tracks for additive manufacturing applications

December 29, 2021
Author(s)
Nicholas Derimow, Edwin Schwalbach, Jake Benzing, Jason Killgore, Aly Artusio-Glimpse, Nik Hrabe, Brian Simonds
In this work, the fundamental processing-structure-property (PSP) relationships that govern laser-based additive manufacturing were investigated with the Ti-6Al-4V alloy. X-ray synchrotron imaging carried out in conjunction with in-situ integrating sphere

Perspectives in Scanning Probe Microscopy from the 2021 Joint International Scanning Probe Microscopy and Scanning Probe Microscopy on Soft and Polymeric Materials Conference

November 30, 2021
Author(s)
Liam Collins, Jason Killgore, Samuel Berweger, Rachael Cohn, neus domingo, Georg Fantner, Rajiv Giridharagopal, Sergei Kalinin, Philippe LECLERE, Simon Scheuring, Rama Vasudevan, Dalia Yablon
In March 2020 our plans for organizing and hosting one of the premier scanning probe microscopy (SPM) conferences in Breckenridge, Colorado, USA were well underway. For the first time the meeting would synergistically combine International Scanning Probe

Microscale Photopatterning of Through-thickness Modulus in a Monolithic and Functionally Graded 3D Printed Part

December 24, 2020
Author(s)
Asais C. Uzcategui, Callie I. Higgins, John Hergert, Andrew Tomaschke, Victor Crespo-Cuevas, Virginia L. Ferguson, Stephanie Bryant, Robert R. McLeod, Jason Killgore
3D printing is transforming traditional processing methods in applications ranging from tissue engineering to optics. To fulfill its maximum potential, 3D printing requires a robust technique for producing structures with precise three-dimensional (x, y