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Search Publications by: Stephen Wise (Assoc)

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Displaying 51 - 75 of 822

Development of Standard Reference Material (SRM) 2973 Vitamin D Metabolites in Frozen Human Serum (High Level)

July 24, 2017
Author(s)
Susan Tai, Michael Nelson, Brian Lang, Karen W. Phinney, Lane C. Sander, James H. Yen, J. M. Betz, Christopher T. Sempos, Stephen Wise
The National Institute of Standards and Technology (NIST), in collaboration with the National Institutes of Health, Office of Dietary Supplements (NIH-ODS) and the Vitamin D Standardization Program (VDSP), has recently issued a new serum-matrix Standard

Qualitative characterization of SRM 1597a Coal Tar for polycyclic aromatic hydrocarbons and methyl-substituted derivatives via normal-phase liquid chromatography and gas chromatography/mass spectrometry

June 29, 2017
Author(s)
Walter Wilson, Hugh Hayes, Lane Sander, Andres Campiglia, Stephen Wise
A normal-phase liquid chromatography (NPLC) fractionation procedure was developed for the characterization of a complex mixture of polycyclic aromatic hydrocarbons (PAHs) from a coal tar sample (Standard Reference Material (SRM) 1597a). Using a semi

Revisiting Shape Selectivity in Liquid Chromatography for Polycyclic Aromatic Hydrocarbons (PAHs) - Six-Ring and Seven-Ring Cata-condensed PAH Isomers of Molecular Mass 328 Da and 378 Da

June 28, 2017
Author(s)
Jorge O. Ona Ruales, Lane C. Sander, Walter Brent Wilson, Stephen Wise
The relationship of reversed-phase liquid chromatography retention on a polymeric C18 stationary phase and the shape of polycyclic aromatic hydrocarbons (PAHs) was investigated for three-ring to seven-ring cata-condensed isomers. We report the first

Normal-phase liquid chromatography retention behavior of polycyclic aromatic hydrocarbon and their methyl-substituted derivatives on an aminopropyl stationary phase

June 16, 2017
Author(s)
Walter Wilson, Hugh Hayes, Lane Sander, Andres D. Campiglia, Stephen Wise
Retention indices for 124 polycyclic aromatic hydrocarbons (PAHs) and 62 methyl-substituted (Me-) PAHs were determined using normal-phase liquid chromatography (NPLC) on a aminopropyl (NH2) stationary phase. PAH retention behavior on the NH2 phase is

Development of an Improved Standard Reference Material for Vitamin D Metabolites in Human Serum

April 4, 2017
Author(s)
Karen W. Phinney, Susan S. Tai, Mary Bedner, Johanna Camara, Rosalind R. Chia, Lane C. Sander, Katherine E. Sharpless, Stephen A. Wise, James H. Yen, Rosemary L. Schleicher, Madhulika Chaudhary-Webb, Khin L. Maw, Yasamin Rahmani, Hubert W. Vesper, Joseph M. Betz, Joyce Merkel, Christopher T. Sempos, Paul M. Coates, Ramon Durazo-Arvizu, Kurtis Sarafin, Stephen P. Brooks

Retention behavior of alkyl-substituted polycyclic aromatic sulfur heterocycle isomers in gas chromatography on stationary phases of different selectivity

January 10, 2017
Author(s)
Walter B. Wilson, Lane C. Sander, Jorge O. Ona Ruales, Stephanie Mossner, Leonard M. Sidisky, Milton Lee, Stephen A. Wise
Retention indices for 10 sets of alkyl-substituted polycyclic aromatic sulfur heterocycles (PASHs) isomers (total of 80 PASHs) were determined using gas chromatography with three different stationary phases: a 50% phenyl phase, a 50% liquid crystalline

Retention behavior of isomeric polycyclic aromatic sulfur heterocycles in gas chromatography on stationary phases of different selectivity

January 10, 2017
Author(s)
Walter B. Wilson, Lane C. Sander, Jorge O. Ona Ruales, Leonard M. Sidisky, Milton Lee, Stephen A. Wise
Retention indices for 70 polycyclic aromatic sulfur heterocycles (PASHs) were determined using gas chromatography with three different stationary phases: a 50% phenyl phase, a 50% liquid crystalline dimethylpolysiloxane (LC-DMPS) phase, and an ionic liquid

The influence of the aromatic character in the gas chromatography elution order: the case of polycyclic aromatic hydrocarbons

November 8, 2016
Author(s)
Jorge O. Ona Ruales, Walter B. Wilson, Federica Nalin, Lane C. Sander, Patricia Schubert, Stephen A. Wise
A link between the aromatic character of polycyclic aromatic hydrocarbons (PAHs) and gas chromatography (GC) elution order in columns with a polysiloxane backbone in the stationary phase is reported for the first time. The aromatic character was calculated

Interlaboratory Analytical Comparison of Fatty Acid Concentrations in Serum or Plasma

September 20, 2016
Author(s)
Michele M. Schantz, Carissa Powers, Schleicher Rosemary, Joseph Betz, Stephen A. Wise
The National Institute of Standards and Technology, in collaboration with the National Institutes of Health Office of Dietary Supplements and the Centers for Disease Control and Prevention, is conducting an accuracy-based program for improving the

Summary of results from the 2014/2015 Hydrocarbon Intercalibration Experiment (HIE)

May 27, 2016
Author(s)
Christopher Reddy, Stephen Wise, Lane C. Sander, Jacolin Murray
Following an open meeting entitled, "Hydrocarbon Chemistry QA/QC," at the 2014 Gulf of Mexico Oil Spill and Ecosystem Science Conference in Mobile, Alabama, the Gulf of Mexico Research Initiative (GoMRI) initiated the Hydrocarbon Intercalibration